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The Mazarites are the main antagonists of the Enterprise episode "Fallen Hero". They were a corrupt species ruled by criminal elements.
The Mazarite political system was notoriously corrupt, with a criminal organisation having control of all levels of government. In an attempt to purge these elements, Vulcan Ambassador V'Lar was sent to Mazar to gather evidence. So she could be kept safe on Vulcan prior to the trial, it was announced that she had been disgraced and was being recalled. Enterprise was sent to pick her up and deliver her to the Vulcan ship Sh'Raan.
However, the Mazarite criminals learned the truth and sent a ship after her. The captain initially attempted to convince Archer to hand V'Lar over, saying she was needed back on Mazar. When Archer was reluctant to comply, the Mazarite ship opened fire on Enterprise. Enterprise managed to disable the ship's engines and escape.
Three Mazarite ships then pursued Enterprise, chasing the Starfleet ship as all vessels pushed their engines to the limit. The Mazarites eventually managed to catch Enterprise and disable it. Stalling for time, Archer claimed they had no working shuttles to transfer V'Lar to them. The Mazarite captain led a boarding party over, where Archer, T'Pol and Phlox convinced them that V'Lar had been injured during the attack and was being treated in an imaging chamber. The Mazarite captain promptly opened fire on the chamber.
At that moment, the Sh'Raan arrived on the scene, with V'Lar and the Enterprise crew having managed to get a message to the Vulcans through the Mazarites' jamming, and easily defeated the Mazarite ships, threatened to destroy them if the Mazarites on Enterprise didn't surrender their weapons to the crew. The Mazarite captain complied, believing they had achieved their objective and killed V'Lar...only for V'Lar to walk in, revealing the imaging chamber had been empty and that she now had more evidence against them. The Mazarites were then allowed to leave.
The Mazarite captain was played by John Rubinstein.